Melamine
Formula:C3H6N6
Mol. Welght:126.12
CAS No.:108-78-1
Storage Temperature:20℃±4℃
Storage and handling:The RM should be stored in the original sealed bottle at the temperature given above.After use the bottle should be tightly closed and protected from moisture .
Purity:99.44% (g/g)
Expanded Uncertainty U= 0.43% (g/g)
The uncertainty of this standard is calculated in accordance with the lSO Guide 34 and EURACHEM/CITAC Guide - Quantifying Uncertainty in Analytical Measurement, Second Edition.The expanded uncertainty is U(exp)=u(RM)x k, where k is the coverage factor at the 95% confidence level (k=2). Uncertainty u(RM)is based on the combination of the uncertainties associated with each indvidual operation involved in the analysis of the product u(RM)=vu(char)2+u(bb)2+u(lts)2+u(sts)2; u(char) is the uncertainty of charactersation; u(bb) uncertainty of homogeneity test;u(lts) uncertaintyof stability test long-term; u(sts) uncertainty of stablitytest short-term.u(lts) and u(sts) are not incuded in the calculation as the stablity statement is based on real evidence opposed to simulation.
Minimum sample: 1 mg is recommended as the minimal sample amount.If less material is used it is recommended to increase the ceritfied uncertainty by a factor of two for half sample and a factor of four for a quarter of sample.
Intended use: Use this RM as calibrant for chromatography or any other analytical technique.
Analytical Data
Traceabity of dhromatography: To the intemational System of Units (SI).
Instrumert:HPLC/DAD
Detectionc:DAD
Column:Nucledur 100 C8 3 um 250x4 mm
lnj.-VolL:3 μl
Flow:1.0 mL/min
Ret.Time:1.72min
Method Details
Eluent A: Acetonitrile:H20+0.5% H3PO4 1:9 for 1 min
Eluent B: Acetonitrile:100% for 5 min
Eluent A -> Eluent B: 19 min
Comment
Traceabity: The balances used are calibrated with weights traceable to the national standards (DKD).
Calibnated dass A glassware is used for volumetric measurements.
Water Content:<0.10% (g/g) by Karl-Fischer-Titration (U(exp) = 0.03% (g/g)).
Purity was determined by elemental analysis
ldentity:EA, NMR RT, IR,UV, MS
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