1.0 ACCREDITATION / REGISTRATION
INORGANIC VENTURES is accredited to ISO Guide 34, "General Requirements for the Competence of Reference Material Producers" and ISO/IEC 17025, "General Requirements for the Competence of Testing and Calibration Laboratories". Inorganic Ventures is also an ISO 9001 registered manufacturer (SAI Global File Number 010105).
2.0 PRODUCT DESC RIPTION
Product Code: Single Analyte Atomic Absorption Solution
Catalog Number:AAAU1
Matrix:10% (v/v) HCI
Value 1 Analyte(s):1 000 μg/mL ea:Gold
3.0 CERTIFIED VALUES AND UNC ERTAINTIES
Certified Value:1000土10 μg/mL
Certified Density:1.019 g/mL (measured at 20±1 °C)
4.0 TRACEABILITY TO NIST
The concentration of this solution standard has been venified by Inductively Coupled Plasma Spectroscopy (ICP) and is traceable to NIST SRM 3121
4.1 Thermometer Calibration
- All thermometers are NIST traceable through themometers that are calibrated by an accredited calibration laboratory.
4.2 Balance Calibration
- All analytical balances are calibrated by an accredited calibration laboratory and procedure. The weights used for testing are annually compared to master weights and are traceable to NIST.
4.3 Glassware Calibration
- An in-house procedure is used to calibrate all Class A glassware used in the manufacturing and quality control of CRM/RMs.
5.0 TRACE METALLIC IMPURITIES (TMI ) DETERMINED BY ICP-MS AND ICP-OES (ug/mL)
N/A
6.0 INTENDED USE
.- For the calibration of analytical instruments and validation of analytical methods as appropriate.
7.0 INSTRUCTIONS FOR THE CORRECT USE OF THIS REFERENCE MATERIAL
7.1 Storage and Handling Recommendations
- Store between approximately 4° - 30℃ while in sealed TCT bag.
- While stored in the sealed TCT bag, transpiration of this CRM/RM is negligible. After opening the sealed TCT bag transpiration of the CRM/RM will occur, resulting in a gradual increase in the analyte concentration(s). It is the responsibility of the user to account for this effect. When the bottle is weighed both before and after being placed in storage, the mass difference observed will be a measure of transpiration mass loss.
. After opening the sealed TCT bag keep cap tightly sealed when not in use. Store and use at 20°土4°℃. Do not pippette from the container. Do not return removed aliquots to container.
- For more information, visit
Atomic Weight; Valence; Coordination Number; Chemical Form in Solution - 196.97 +3 6 Au(CI)63 Chemical Compatibility -Stable in HCI, and HNO3, as the chloride complex. Avoid basic media. Stable with most metals and inorganic anions in acidic media.
Stability - 2-100 ppb levels. 2-10 ppb Au is stable for #1day maximum in 1% HNO3 / LDPE container. 100 ppb is stable for #2 days maximum in 1% HNO3 / LDPE container.1-10,000 ppm solutions chemically stable for years in 10% HCI 1 LDPE container.
Au Containing Samples (Preparation and Solution) - Metal (Aqua Regia ); Oxides ( Soluble in HCI ); Ores (Dissolve in HCI / HNO3).
Atomic Spectroscopic Information (ICP-OES D.L.s are given as radial/axial View):
Technique/Line |
Estimated D.L. |
Order |
Interferences (underlined indicates severe) |
ICP-MS 197 amu |
5 ppt |
N/A |
181Ta 160 |
ICP-OES 208.209 nm |
0.04/0.01 ug/mL |
1 |
Ir, Re |
ICP-OES 242.795 nm |
0.02/0.003 μg/mL |
1 |
Mn, Os, Th, Ta, Pt,Co, F |
ICP-OES 267.595 nm |
0.03/0.003 ug/mL |
1 |
Nb, Ta,U, Cr, Th,Rh, Ru |
8.0 HAZARDOUS INFORMATION
- Please refer to the Safety Data Sheet for information regarding this CRM/RM.
9.0 HOMOGENEITY
- This solution was mixed according to an in-house procedure and is guaranteed to be homogeneous. Homogeneity data indicate that the end user should take a minimum sample size of 0.2 mL to assure homogeneity.
10.0 QUALITY STANDARD DOCUMENTATION
10.1 10CFR50 Appendix B - Nuclear Regulatory Commission
Domestic Licensing of Production and Utilization Facilities
10.2 10CFR21 - Nuclear Regulatory Commission
- Reporting defects and Non-Compliance
10.3 ISO 9001 Quality Management System Registration
- SAI Global File Number 010105
11.0 CERTIFICATION, LOT EXPIRATION AND PERIOD OF VALIDITY
11.1 Certification Issue Date
January 26, 2016
- The certification is valid within the measurement uncertainty specified provided the CRM/RM is stored and handled in accordance with instructions given in Sec 7.1. This certification is nulified if instructions in Sec 7.1 are not followed or if the CRM/RM is damaged, contaminated, or otherwise modified.
11.2 Lot Expiration Date
- January 26, 2020
- The date after which this CRM/RM should not be used.
- The lot expiration date reflects the period of time that the stability of a CRM/RM can be supported by long term stability studies conducted on properly stored and handled CRM/RMs. Lot expiration is limited primarily by transpiration (loss of water from the solution) and infrequently by chemical stability.
11.3 Period of Validity
. Sealed TCT Bag Open Date:
- This CRM/RM should not be used longer than one year from the date of removal from the aluminized bag or afer the date given in Sec.11 .2, whichever comes first. This is contingent upon the CRM/RM being handled and stored in accordance with the instructions given in Sec 7.1.
注:证书信息仅供参考,以产品附带证书为准。