PRODUCT DESCRIPTION
Product Code: Single Analyte Atomic Absorption Solution
Catalog Number: AACO1
Lot Number: K2-CO02072
Matrix: 3% (v/v) HNO3
Value / Analyte(s):
1 000 µg/mL ea:
Cobalt
CERTIFIED VALUES AND UNCERTAINTIES
Certified Value: 1000 ± 10 μg/mL
Certified Density: 1.020 g/mL (measured at 20 ± 1 ºC)
TRACEABILITY TO NIST
The concentration of this solution standard has been verified by Inductively Coupled Plasma Spectroscopy (ICP) and is traceable to NIST SRM 3113
1.Thermometer Calibration
-All thermometers are NIST traceable through thermometers that are calibrated by an accredited calibration laboratory.
2.Balance Calibration
-All analytical balances are calibrated by an accredited calibration laboratory and procedure. The weights used for testing are annually compared to master weights and are traceable to NIST.
3.Glassware Calibration
-An in-house procedure is used to calibrate all Class A glassware used in the manufacturing and quality control of CRM/RMs
TRACE METALLIC IMPURITIES (TMI ) DETERMINED BY ICP-MS AND ICP-OES (µg/mL)
N/A
INTENDED USE
For the calibration of analytical instruments and validation of analytical methods as appropriate
NSTRUCTIONS FOR THE CORRECT USE OF THIS REFERENCE MATERIAL
1.Storage and Handling Recommendations
-Store between approximately 4° - 30° C while in sealed TCT bag.
-While stored in the sealed TCT bag, transpiration of this CRM/RM is negligible. After opening the sealed TCT bag transpiration of the CRM/RM will occur, resulting in a gradual increase in the analyte concentration(s). It is the responsibility of the user to account for this effect. When the bottle is weighed both before and after being placed in storage, the mass difference observed will be a measure of transpiration mass loss.
-After opening the sealed TCT bag keep cap tightly sealed when not in use. Store and use at 20° ± 4° C. Do not pippette from the container. Do not return removed aliquots to container.
Atomic Weight; Valence; Coordination Number; Chemical Form in Solution - 58.93 +2 6 Co(H2O)62+
Chemical Compatibility -Stable in HCl, HNO3, H2SO4 ,HF, H3PO4. Avoid basic media. Stable with most metals and inorganic anions in acidic media.
Stability - 2-100 ppb levels stable for months in 1% HNO3 / LDPE container. 1-10,000 ppm solutions chemically stable for years in 1-5% HNO3 / LDPE container.
Co Containing Samples (Preparation and Solution) - Metal (soluble in HNO3 ); Oxides ( Soluble in HCl ); Ores (dissolve in HCl / HNO3).
Atomic Spectroscopic Information (ICP-OES D.L.s are given as radial/axial view):
Technique/Line
|
Estimated D.L. |
Order |
Interferences (underlined indicates severe) |
ICP-MS 59 amu
|
2 ppt
|
n/a
|
42Ca16O1H ,
|
|
|
|
40Ar18O1H ,
|
|
|
|
36Ar23Na,
|
|
|
|
43Ca16O,
|
ICP-OES 228.616 nm
|
0.01/0.001 µg/mL
|
1
|
24Mg35Cl
|
ICP-OES 237.862 nm
|
0.01/0.002 µg/mL
|
1
|
W, Re, Al, Ta
|
ICP-OES 238.892 nm
|
0.01/0.002 µg/mL
|
1
|
Fe, W, Ta
|
HAZARDOUS INFORMATION
-Please refer to the Safety Data Sheet for information regarding this CRM/RM.
HOMOGENEITY
-This solution was mixed according to an in-house procedure and is guaranteed to be homogeneous. Homogeneity data indicate that the end user should take a minimum sample size of 0.2 mL to assure homogeneity.
QUALITY STANDARD DOCUMENTATION
1.10CFR50 Appendix B - Nuclear Regulatory Commission
- Domestic Licensing of Production and Utilization Facilities
2.10CFR21 - Nuclear Regulatory Commission
-Reporting defects and Non-Compliance
3.ISO 9001 Quality Management System Registration
-QSR Certificate Number QSR-1034
CERTIFICATION, LOT EXPIRATION AND PERIOD OF VALIDITY
注:证书信息仅供参考,以产品附带证书为准。